E – 02 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys, cobalt alloys. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by. ASTM E Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel, Iron, Nickel, and Cobalt Alloys by Various Combustion.
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NOTE 17—If the samples are to be analyzed in the automatic mode, blank determination and calibration should also be performed in the automatic mode. Additional elements not included in the table will cause extra cost.
Prepare the number of replicates indicated and then proceed as directed in Users of this test method are cautioned that use of it above 0. NOTE 23—If the unit does not have this function, the wstm value must be subtracted from the total result prior to any calculation. Summary of Test Method Reports are provided according to the elements in question.
It is therefore recommended that calibrants be of the same or similar composition as the samples to be analyzed. This standard is not included in asttm packages. It is assumed 1.
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Analyses of C, S, N and O by combustion and fusion techniques Analyses of H by fusion technique For scopes outside specified limit, please inquire. Remove from the furnace and cool in air for 90 6 15 s before use. NOTE 33—Although these test methods were tested to only 0.
Each gas is measured with a solid state energy detector. Subscription pricing is determined by: Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM International Headquarters. Test Method C—The detector consists of an IR energy source, a separate measure chamber and reference chamber, and a diaphragm acting as one plate of a parallel plate capacitor. Additional elements not included in the table requires a separate inquire.
NOTE 1—The accelerator should contain no more than 0. In this case, laboratories should perform method validation using reference materials.
Note 22—The upper limit of the scope has been set at 0. For smaller sizes, please contact us. Thus, the absorption of IR energy can be attributed to only CO2 and its concentration is measured as changes in energy at the detector.
Use Calibrant CCC as the primary calibrant and analyze at least three test samples to determine the calibration slope. We have no amendments or corrections for this standard. Remove from furnace and cool in air for 90 6 15 s before use. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard.
Apparatus and Reagents 5. Standards Subscriptions from ANSI provides a money-saving, multi-user solution for accessing standards. This mechanism will electronically compensate for the blank value. This mechanism will electronically compensate for the blank value Note Energy from the IR source passes through both chambers, simultaneously arriving at the diaphragm capacitor plate.
If not, repeat The scopes are reviewed annually by Swedac. Already Subscribed to this document. For some material, such as plain carbon sheet steel, a rimmed or semi-killed deoxidation practice is used and the oxygen may not be uniformly distributed throughout the thickness of the sample.
NOTE 26—The accelerator should contain no more than 0. As the voice of the U. To each, add 1. If necessary, wash three times with acetone by decantation to remove organic contaminants and dry at room temperature.
Test the furnace and the analyzer to ensure the absence of leaks. Need more than one copy? You may delete a document from your Alert Profile at any time. A number in parentheses indicates the year of last reapproval.
The value should agree with the assigned value for Calibrant C within a range of 6 s, the standard deviation of a single determination of Calibrant C using this method. Adjust the signal to provide a reading within The use of small and irregular shaped sstm requires a diligent effort to ensure that all surface contamination has been removed.
We can analyse your samples of Fe-base Ni-base Cu-base Al-base Co-base Ti-base Our advanced analyses equipment, duplicated to ascertain high delivery reliability, contains i a the most advanced spectrometers available on the market. NOTE 16—Repeat the calibration when: Note 12—The upper limit of the scope has been set at 0.